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Go to Editorial ManagerThis study is focused on the assessment of the effects of Sulphur percentage in submerged arc welded API 5L X60 steel under conditions simulated to crude oil environments on its mechanical properties and microstructure. This involved immersing welded specimens in distilled water containing high (0.3250 ml/4L distilled water) and low (0.25 ml/4L distilled water) Sulphur concentrations for four weeks, while unimmersed samples were used as controls for comparison between the two groups of samples. The related experiments were tensile test, hardness measurements, SEM and EDS analyses and XRD analysis. The most mechanically degraded was the high- Sulphur group (H-group); yield strength of 441 MPa (17% loss) and ultimate tensile strength of 506 MPa (11% loss). For the low-sulfur group (L-group), reductions were more moderate: 467 MPa and 523 MPa, respectively. Weld metal (WM) and HAZ hardness values in the H-group were 203 HB and 208 HB, respectively, while those of the L-group were 208 HB and 214 HB. The H-group created a non-protective mixed layer of acicular iron oxides and iron sulfides (FeS) with respect to the microstructural aspects, whereas the L-group developed a thin protective film of iron oxide free from sulfides. Welding parameters were investigated for their effect on the corrosion rate and mechanical properties.
Zinc and its alloy coatings are commonly used to provide cathodic protection for weathering steel. However, the steel substrate corrodes faster than the Zinc coating because of the coating's negative corrosion potential. Many studies have examined Zinc and alloy coatings' resistance to corrosion. Hot-dip galvanizing, Electrodeposition, and Zinc-rich coat (ZRC) spray are just some of the methods that can be used to deposit such coatings. Commercially available 99.95 % pure Zinc oxide was used in the electroplating process in this investigation. Steel samples were plated in Zinc sulphate and Zinc oxide solutions and were controlled by different bath parameters such as voltage, current, pH, temperature, and coating time. The addition of hexagonal Boron Nitride (h-BN) nanoparticles has also shown significant improvements in corrosion resistance. However, Zinc-based coating techniques reinforced with h-BN incorporation show the best corrosion current density ( I corr ) of Hot dip 2 % wt. (2.1 µA/cm 2 ), ZRC 2.5 % wt., (4.4 µA/cm 2 ), and electroplating 15.75 g/L (0.081 µA/cm 2 ), which is an order of magnitude lower than coatings without h-BNs. The corrosion rates and current densities of Zn/h-BN coated layers were investigated in a controlled laboratory environment that mimicked natural conditions (Rainwater solution) by extrapolating polarization curves.
The aim of this study is to investigate the effect of heat treatments on the impact properties of hot rolled high strength steel and describes the effect of tempering temperature and quenching media on the microstructure, hardness, and impact resistance of plates. In the present study a high strength steel was austenitized at 900 °C with different quenching medium and followed by tempering at 300 °C, 500 °C. After thermal treatments, the values of Charpy impact resistance, hardness, and microscopic structure were evaluated from mechanical and metallographic analysis of metals respectively. The change of mechanical properties and microstructure of the metal with the existence of heat treatment with the ballistic performance of high-strength steel. Experimental results showed that tempering at 500 °C for 2 hours after water quenching medium it provides the best mechanical properties in conjunct on with an improved in microstructure.
The enormous volume of crude oil that needs to be transported results from the growing demand for petroleum. One of the most practical ways to move crude oil is via pipelines. This paper's primary objective is to examine the effects of sulphur, one of the components of crude oil, on welded pipes (API 5L X60, X46, and X42 pipes as well as ASTM A106 pipes). It also aims to show how sulphur content influences different kinds of pipes separately from the other important components of crude oil. The sulphur content of crude oil is determined using the TR-TCXRF equipment. The corrosion rates of welded pipes in four immersion solutions (Different percentages of sulphur content) were computed using weight loss. The samples' corrosion characteristics were assessed morphologically using an optical microscope (OM), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). Petroleum welded pipelines' mechanical qualities and resistance to corrosion are significantly impacted by sulphur; an increase in sulphur concentration resulted in a higher rate of corrosion and a decrease in mechanical properties. Among all the welded pipes utilized in the paper, the API 5L X60 welded pipe had the highest corrosion rate, whereas X46 welded pipe was more corrosion-resistant than X46 and X42 in API 5L-type pipes and ASTM A106 pipe.